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Oxidation Chemistry of Inorganic Benzene Complexes

Fleischmann, Martin ; Dielmann, Fabian ; Balázs, Gábor ; Scheer, Manfred


The oxidation of the 28 VE cyclo-E-6 triple-decker complexes [((CpMo)-Mo-R)(2)(mu,eta(6):eta(6)-E-6)] (E = P, Cp-R = Cp(2a), Cp*(2b), Cp-Bn(2c)= C-5(CH2Ph)(5); E = As, Cp-R = Cp*(3)) by Cu+ or Ag+ leads to cationic 27 VE complexes that retain their general triple-decker geometry in the solid state. The obtained products have been characterized by cyclic voltammetry ( CV), EPR, Evans NMR, ...


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