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Ring Expansions of Nonpolar Polyphosphorus Rings

Piesch, Martin ; Seidl, Michael ; Stubenhofer, Markus ; Scheer, Manfred


The reaction of the phosphinidene complex [Cp*P{W(CO)(5)}(2)] (1a) (Cp*=C5Me5) with the anionic cyclo-Pn ligand complex [(eta(3)-P-3)Nb(ODipp)(3)](-) (2, Dipp = 2,6-diisopropylphenyl) resulted in the formation of [{W(CO)(5)}(2){mu(3),eta(3:1:1)-P4Cp*}Nb(ODipp)(3)](-) (3), which represents an unprecedented example of a ring expansion of a polyphosphorus-ligand complex initiated by a phosphinidene ...


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