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Tetraglymes as Prochiral Host Reagents for Ammonia Borane

Shelyganov, Pavel A. ; Virovets, Alexander ; Peresypkina, Eugenia ; Scheer, Manfred ; Timoshkin, Alexey Y.


The molecular structure of the complex of ammonia borane (AB) with acyclic ether tetraglyme Me(OCH2CH2)(4)OMe (1), 1(AB)(2) was determined by single-crystal X-ray structure analysis for the first time. The crystal structure features two AB molecules, bonded by dihydrogen bonds, per one tetraglyme unit. The intermolecular BHHN distances of 1.94 angstrom are shorter than those in the solid ammonia ...


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