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The benefits of Cu Kβ radiation for the single-crystal X-ray structure determination of crystalline sponges

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Meurer, Florian ; von Essen, Carolina ; Kühn, Clemens ; Puschmann, Horst ; Bodensteiner, Michael
License: Creative Commons Attribution 4.0
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Date of publication of this fulltext: 05 Apr 2022 04:56


The crystalline sponge method facilitates the X-ray structure determination of samples that do not crystallize or are too sparsely available to afford viable crystallization. By including these materials in a metal-organic framework, the structure of the guest molecules can be determined. Some of the inherent difficulties of this method are discussed and the use of Cu K beta radiation is ...


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