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The benefits of Cu Kβ radiation for the single-crystal X-ray structure determination of crystalline sponges

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Meurer, Florian ; von Essen, Carolina ; Kühn, Clemens ; Puschmann, Horst ; Bodensteiner, Michael
License: Creative Commons Attribution 4.0
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Date of publication of this fulltext: 05 Apr 2022 04:56


The crystalline sponge method facilitates the X-ray structure determination of samples that do not crystallize or are too sparsely available to afford viable crystallization. By including these materials in a metal–organic framework, the structure of the guest molecules can be determined. Some of the inherent difficulties of this method are discussed and the use of Cu Kβ radiation is presented as ...


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