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Activation of Di‐tert‐butyldiphosphatetrahedrane: Access to (tBuCP)n (n=2, 4) Ligand Frameworks by P−C Bond Cleavage

Hierlmeier, Gabriele ; Wolf, Robert


The first mixed phosphatetrahedranes were reported only recently and their reactivity is virtually unexplored. Herein, we present a reactivity study on di-tert-butyldiphosphatetrahedrane (1), which is the dimer of tert-butylphosphaalkyne. The (tBuCP)(2) tetrahedron is activated selectively by N-heterocyclic carbene (NHC) nickel(I) and nickel(0) complexes, resulting in novel complexes featuring ...


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